返回 2008年第31卷第3期 目录

复方岗松洗液的薄层色谱研究

傅秀娟

（泸州医学院药学院，四川泸州 646000）

摘 要 目的：对复方岗松洗液中的药材进行定性研究，以便更好地控制产品质量。方法：对方中主要药味苦豆草、岗松、黄柏、冰片、红花五味药用薄层色谱法进行定性研究，展开系统分别为苯-丙酮-醋酸乙酯(7∶3∶3)、石油醚(60℃～90℃) -醋酸乙酯(5∶1)、苯-醋酸乙酯(19∶1)、正丁醇-冰醋酸-水(7∶1∶2)及环已烷－乙酸乙酯（5∶3）。结果：供试品色谱在对照品或对照药材色谱相应位置上显相同颜色斑点，所得斑点清晰，专属性强，重现性好，分离度良好，阴性样品无干扰。结论：所建立的方法简便、结果准确、重复性好，可用于产品的质量控制。

关键词 复方岗松洗液；薄层色谱；苦豆草；岗松；黄柏；冰片；红花

THE TLC INVESTIGATION OF COMPOUND GANGSONG LOTION

Fu Xiujuan

Department of Pharmacy,Luzhou Medical College

Abstract Objective: To carry out the qualitative investgation into the ingredient of compound GangSong Lotion, in order to improve the quality control over the products. Methods: TLC was applied to identify Herba Sophorae alopecuroidis, baeckea frutescens linn, Phellodendron chinense schneid, borneolum syntheticum and carthamus tinctorius. And the development systems were as follows: benzene-actone-ethyl acetate (7∶3), petrolem ether (60℃～90℃)-ethyl acetate (5:1), benzene-ethyl acetate (19∶1), n-butanol-acetic acid-aquar (7∶1∶2), hexamethylene-ethyl acetate(5∶3). Results:The chromatography of the samples clearly presented the same-colored spots as the chromatography of the reference herbs. Thus this method was considered to be specific, reproductive, fine in resolving power and no interference of the negative samples. Conclusion: The established method is simple, accurate, reproductive and can be used for quality controlment.

Key words Compound GangSong lotion; TLC; Herba Sophorae Alopecuroidis; Baeckea frutescens linn, Phellodendron chinense schneid; Borneolum syntheticum; Carthamus tinctorius